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Table 3. Complete composition and extraction yield (% w/w dry weight) of the essential oil obtained from the dried inflorescences and floral bracts of 2020 hemp samples. 1 LRI = Linear retention index on a HP 5-MS capillary column; 2 Not detected; 3 Compounds accounting for at least 1.000% of the dissimilarity rate (according to the SIMPER test; see Table 4) are evidenced in bold. For these compounds, for all chemical classes, and for the extraction yield, different superscript uppercase letters (A–G) indicate statistically significant differences between each variety; superscript lowercase letters (a,b) indicate statistically significant differences among the cultivar withdrawn on different years (see Table 2 for 2019 samples). The statistical significance of the relative abundances was established by the Tukey’s post-hoc test, with p ≤ 0.05.
|
Relative abundance (%) ± SD
|
Compounds
|
LRI1
|
Monoecious
|
Dioecious
|
Carmaleonte
|
Codimono
|
Felina 32
|
Futura 75
|
Uso-31
|
Bernabeo
|
Carmagnola
|
CS
|
Eletta Campana
|
Fibranova
|
Fibrante
|
heptanal
|
901
|
-2
|
-
|
-
|
-
|
-
|
0.3 ± 0.06
|
0.1 ± 0.10
|
0.1 ± 0.04
|
0.1 ± 0.07
|
-
|
-
|
α-pinene3
|
933
|
2.7 ± 0.50AB;a
|
2.0 ± 0.74ABC;a
|
1.1 ± 0.40CD;a
|
1.1 ± 0.11CD;a
|
2.0 ± 0.26ABC;a
|
0.5 ± 0.06D;a
|
3.0 ± 0.04A;a
|
2.1 ± 0.79ABC;a
|
1.7 ± 0.01BC;a
|
1.3 ± 0.39CD;a
|
1.2 ± 0.06CD;a
|
β-pinene
|
977
|
0.5 ± 0.06
|
0.5 ± 0.17
|
0.3 ± 0.07
|
0.2 ± 0.06
|
0.7 ± 0.18
|
0.1 ± 0.01
|
0.8 ± 0.09
|
0.7 ± 0.26
|
0.5 ± 0.02
|
0.3 ± 0.12
|
0.4 ± 0.03
|
myrcene3
|
991
|
0.8 ± 0.09CD;a
|
0.8 ± 0.33CD;a
|
0.2 ± 0.02D;a
|
0.4 ± 0.09D;a
|
0.6 ± 0.12D;a
|
0.4 ± 0.05D;a
|
2.6 ± 0.16A;a
|
1.3 ± 0.49BC;a
|
0.6 ± 0.01D;a
|
0.3 ± 0.10D;a
|
1.8 ± 0.17B;a
|
δ-3-carene
|
1011
|
0.1 ± 0.05
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.01
|
0.3 ± 0.09
|
-
|
α-terpinene
|
1017
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.06
|
-
|
-
|
-
|
limonene
|
1029
|
0.1 ± 0.01
|
0.1 ± 0.08
|
-
|
-
|
0.2 ± 0.01
|
0.1 ± 0.03
|
0.6 ± 0.10
|
0.7 ± 0.16
|
0.4 ± 0.01
|
0.1 ± 0.08
|
0.8 ± 0.08
|
1,8-cineole
|
1031
|
-
|
0.2 ± 0.05
|
-
|
-
|
-
|
0.2 ± 0.05
|
0.2 ± 0.09
|
0.2 ± 0.06
|
0.1 ± 0.02
|
0.2 ± 0.06
|
0.1 ± 0.06
|
(E)-β-ocimene
|
1047
|
0.1 ± 0.01
|
0.4 ± 0.13
|
-
|
0.1 ± 0.03
|
0.4 ± 0.02
|
-
|
0.3 ± 0.02
|
0.1 ± 0.06
|
0.2 ± 0.01
|
0.3 ± 0.07
|
-
|
γ-terpinene
|
1058
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.07
|
-
|
-
|
-
|
terpinolene
|
1089
|
-
|
0.4 ± 0.14
|
0.2 ± 0.04
|
0.1 ± 0.09
|
0.1 ± 0.02
|
0.1 ± 0.01
|
0.3 ± 0.03
|
0.8 ± 0.19
|
0.3 ± 0.01
|
-
|
0.5 ± 0.03
|
nonanal
|
1105
|
0.1 ± 0.07
|
-
|
-
|
-
|
0.1 ± 0.06
|
0.2 ± 0.04
|
-
|
-
|
-
|
-
|
-
|
linalool
|
1101
|
-
|
0.1 ± 0.06
|
-
|
-
|
-
|
-
|
0.2 ± 0.01
|
0.2 ± 0.04
|
0.1 ± 0.03
|
-
|
-
|
fenchol
|
1114
|
-
|
-
|
-
|
-
|
-
|
-
|
0.2 ± 0.02
|
0.4 ± 0.07
|
0.2 ± 0.05
|
-
|
0.3 ± 0.00
|
cis-p-menth-2-en-1-ol
|
1122
|
-
|
-
|
-
|
-
|
-
|
-
|
0.2 ± 0.02
|
0.2 ± 0.03
|
0.2 ± 0.02
|
-
|
0.2 ± 0.01
|
trans-pinocarveol
|
1139
|
0.3 ± 0.03
|
-
|
-
|
-
|
0.1 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
-
|
trans-verbenol
|
1145
|
-
|
-
|
-
|
-
|
0.2 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
-
|
ipsdienol
|
1147
|
|
|
|
|
|
|
|
|
|
|
|
β-pinene oxide
|
1156
|
-
|
-
|
-
|
-
|
-
|
-
|
0.3 ± 0.03
|
-
|
-
|
-
|
0.1 ± 0.01
|
borneol
|
1165
|
0.2 ± 0.02
|
0.1 ± 0.05
|
-
|
-
|
-
|
0.1 ± 0.00
|
0.2 ± 0.02
|
0.2 ± 0.04
|
0.2 ± 0.00
|
0.1 ± 0.06
|
0.2 ± 0.01
|
lavandulol
|
1170
|
-
|
0.4 ± 0.09
|
0.3 ± 0.06
|
0.2 ± 0.05
|
0.2 ± 0.05
|
0.4 ± 0.06
|
0.3 ± 0.01
|
0.6 ± 0.03
|
0.3 ± 0.01
|
-
|
0.6 ± 0.04
|
4-terpineol
|
1177
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.2 ± 0.03
|
-
|
p-cymen-8-ol
|
1185
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
myrtenal
|
1194
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
α-terpineol
|
1191
|
-
|
0.2 ± 0.03
|
-
|
-
|
-
|
0.2 ± 0.04
|
0.3 ± 0.01
|
0.5 ± 0.04
|
-
|
0.2 ± 0.03
|
0.5 ± 0.02
|
eugenol
|
1357
|
0.2 ± 0.06
|
0.1 ± 0.07
|
-
|
0.1 ± 0.03
|
0.1 ± 0.01
|
-
|
-
|
-
|
-
|
0.2 ± 0.07
|
-
|
methyl eugenol
|
1405
|
-
|
-
|
-
|
-
|
0.1 ± 0.02
|
-
|
-
|
-
|
-
|
-
|
-
|
α-ylangene
|
1374
|
0.2 ± 0.01
|
0.1 ± 0.07
|
-
|
0.1 ± 0.01
|
-
|
-
|
0.1 ± 0.04
|
0.1 ± 0.02
|
0.3 ± 0.01
|
0.1 ± 0.07
|
-
|
isocaryophyllene
|
1407
|
0.4 ± 0.03
|
0.4 ± 0.00
|
0.3 ± 0.09
|
0.4 ± 0.03
|
0.2 ± 0.01
|
0.3 ± 0.11
|
0.2 ± 0.04
|
0.3 ± 0.06
|
0.3 ± 0.01
|
0.5 ± 0.12
|
0.3 ± 0.01
|
cis-α-bergamotene
|
1416
|
-
|
0.1 ± 0.01
|
0.4 ± 0.14
|
0.1 ± 0.09
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
β-caryophyllene3
|
1419
|
15.3 ± 1.44AB;a
|
16.2 ± 1.46AB;a
|
11.5 ± 3.55ABC;a
|
13.8 ± 0.59ABC;a
|
8.7 ± 0.77C;a
|
10.4 ± 2.95BC;a
|
14.4 ± 0.89ABC;a
|
15.4 ± 2.45AB;a
|
11.6 ± 0.09ABC;a
|
16.8 ± 3.82A;a
|
16.2 ± 0.8AB;a
|
trans-α-bergamotene
|
1436
|
0.3 ± 0.00
|
1.1 ± 0.04
|
1.6 ± 0.42
|
1.5 ± 0.16
|
1.0 ± 0.06
|
0.3 ± 0.06
|
0.1 ± 0.01
|
0.1 ± 0.08
|
0.3 ± 0.01
|
0.9 ± 0.2
|
-
|
α-guaiene
|
1439
|
-
|
-
|
-
|
-
|
-
|
0.6 ± 0.14
|
-
|
-
|
-
|
-
|
-
|
aromadendrene
|
1142
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.3 ± 0.04
|
-
|
guaia-6,9-diene
|
1443
|
0.2 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.05
|
0.1 ± 0.05
|
-
|
isogermacrene D
|
1451
|
0.3 ± 0.03
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.2 ± 0.01
|
-
|
-
|
α-humulene3
|
1453
|
6.9 ± 1.00ABC;a
|
7.6 ± 0.17A;a
|
4.7 ± 1.23DE;a
|
5.8 ± 0.38ABCDE;a
|
4.1 ± 0.06E;a
|
6.2 ± 0.27ABCD;a
|
5.3 ± 0.10CDE;a
|
7.5 ± 0.19A;a
|
5.4 ± 0.13BCDE;a
|
6.3 ± 1.44ABCD;a
|
7.4 ± 0.38AB;a
|
aristolene
|
1452
|
-
|
-
|
-
|
0.1 ± 0.05
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
(E)-β-farnesene
|
1458
|
0.3 ± 0.04
|
1.2 ± 0.07
|
1.4 ± 0.37
|
1.7 ± 0.19
|
1.1 ± 0.05
|
0.4 ± 0.01
|
0.1 ± 0.07
|
0.1 ± 0.09
|
0.3 ± 0.03
|
0.8 ± 0.19
|
0.1 ± 0.06
|
alloaromadendrene
|
1460
|
0.4 ± 0.07
|
0.9 ± 0.00
|
0.6 ± 0.16
|
0.7 ± 0.07
|
0.9 ± 0.01
|
0.4 ± 0.03
|
0.3 ± 0.03
|
0.5 ± 0.01
|
0.4 ± 0.02
|
0.5 ± 0.09
|
0.2 ± 0.01
|
4,5-di-epi-aristolochene
|
1468
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
γ-gurjunene
|
1469
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
β-chamigrene
|
1476
|
-
|
-
|
-
|
0.1 ± 0.07
|
-
|
0.1 ± 0.03
|
-
|
-
|
-
|
-
|
-
|
γ-muurolene
|
1477
|
0.3 ± 0.02
|
-
|
0.2 ± 0.05
|
0.2 ± 0.04
|
-
|
0.1 ± 0.01
|
-
|
-
|
0.4 ± 0.09
|
0.2 ± 0.04
|
-
|
α-amorphene
|
1482
|
0.2 ± 0.02
|
0.2 ± 0.01
|
0.1 ± 0.02
|
0.2 ± 0.04
|
-
|
0.2 ± 0.01
|
0.1 ± 0.01
|
0.1 ± 0.01
|
0.1 ± 0.03
|
0.1 ± 0.03
|
-
|
γ-selinene
|
1483
|
0.5 ± 0.01
|
0.6 ± 0.04
|
0.5 ± 0.11
|
0.6 ± 0.10
|
0.4 ± 0.01
|
0.6 ± 0.01
|
0.5 ± 0.02
|
0.5 ± 0.03
|
0.5 ± 0.04
|
0.5 ± 0.11
|
0.4 ± 0.01
|
β-selinene3
|
1486
|
1.3 ± 0.03CDE;a
|
1.5 ± 0.10CDE;a
|
2.1 ± 0.48AB;a
|
2.2 ± 0.30A;a
|
1.9 ± 0.02ABC;a
|
1.5 ± 0.08BCDE;a
|
1.2 ± 0.07E;a
|
1.4 ± 0.13CDE;a
|
1.8 ± 0.09ABCD;a
|
1.3 ± 0.31CDE;a
|
1.3 ± 0.05DE;a
|
δ-selinene
|
1491
|
0.2 ± 0.01
|
0.1 ± 0.01
|
-
|
0.2 ± 0.04
|
-
|
0.3 ± 0.03
|
0.2 ± 0.02
|
0.2 ± 0.01
|
0.1 ± 0.04
|
0.1 ± 0.06
|
0.1 ± 0.05
|
valencene
|
1493
|
0.3 ± 0.01
|
0.3 ± 0.03
|
0.2 ± 0.05
|
0.3 ± 0.04
|
0.2 ± 0.00
|
0.3 ± 0.02
|
0.3 ± 0.05
|
0.3 ± 0.02
|
0.2 ± 0.00
|
0.3 ± 0.06
|
0.2 ± 0.02
|
α-selinene
|
1495
|
1.2 ± 0.00
|
1.2 ± 0.04
|
1.7 ± 0.40
|
1.5 ± 0.20
|
0.9 ± 0.09
|
1.5 ± 0.06
|
1.0 ±0.20
|
1.1 ±0.07
|
1.5 ± 0.16
|
1.0 ± 0.26
|
1.0 ± 0.07
|
eremophilene
|
1499
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.04
|
-
|
-
|
-
|
α-bulnesene
|
1505
|
-
|
-
|
-
|
0.1 ± 0.02
|
-
|
1.4 ± 0.04
|
0.2 ± 0.05
|
-
|
0.1 ± 0.03
|
0.1 ± 0.01
|
-
|
epizonarene
|
1501
|
-
|
-
|
-
|
0.2 ± 0.04
|
-
|
-
|
0.2 ± 0.05
|
-
|
0.2 ± 0.03
|
0.2 ± 0.04
|
-
|
β-bisabolene
|
1509
|
0.1 ± 0.00
|
0.3 ± 0.02
|
0.3 ± 0.06
|
0.3 ± 0.04
|
0.2 ± 0.01
|
-
|
-
|
-
|
0.9 ± 0.11
|
0.4 ± 0.09
|
-
|
(E,E)-α-farnesene
|
1509
|
-
|
-
|
-
|
-
|
-
|
0.3 ± 0.01
|
0.4 ± 0.08
|
0.4 ± 0.06
|
-
|
-
|
0.4 ± 0.01
|
β-curcumene
|
1513
|
-
|
0.1 ± 0.01
|
0.2 ± 0.05
|
0.2 ± 0.03
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
trans-γ-cadinene
|
1513
|
0.5 ± 0.01
|
0.1 ± 0.00
|
0.3 ± 0.06
|
0.2 ± 0.01
|
-
|
0.1 ± 0.01
|
-
|
-
|
0.4 ± 0.03
|
0.2 ± 0.03
|
-
|
sesquicineole
|
1516
|
-
|
0.6 ± 0.03
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
7-epi-α-selinene
|
1517
|
0.4 ± 0.37
|
-
|
0.4 ± 0.05
|
0.6 ± 0.08
|
0.3 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
-
|
(Z)-γ-bisabolene
|
1519
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
β-cadinene
|
1519
|
0.3 ± 0.01
|
0.2 ± 0.01
|
-
|
0.1 ± 0.14
|
-
|
0.2 ± 0.01
|
0.2 ± 0.02
|
0.2 ± 0.02
|
0.4 ± 0.05
|
0.3 ± 0.05
|
0.1 ± 0.05
|
trans-calamenene
|
1524
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.05
|
-
|
-
|
-
|
-
|
-
|
δ-cadinene
|
1524
|
0.5 ± 0.03
|
0.4 ± 0.02
|
0.6 ± 0.06
|
0.5 ± 0.07
|
0.2 ± 0.02
|
0.2 ± 0.01
|
0.1 ± 0.01
|
0.2 ± 0.02
|
0.5 ± 0.10
|
0.3 ± 0.07
|
0.1 ± 0.01
|
selina-3,7(11)-diene3
|
1530
|
5.2 ± 0.47BC;a
|
3.2 ± 0.05DE;a
|
2.1 ± 0.65DEF;a
|
3.8 ± 0.55CD;a
|
1.3 ± 0,13F;a
|
3.8 ± 0.26CD;a
|
3.4 ± 0.33DE
|
3.1 ± 0.20DE;a
|
8.6 ± 1.01A;a
|
5.6 ± 1.3B;a
|
1.9 ± 0.09EF;a
|
(E)-γ-bisabolene
|
1531
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
α-calacorene
|
1543
|
0.4 ± 0.05
|
-
|
0.2 ± 0.01
|
0.3 ± 0.03
|
-
|
0.4 ± 0.04
|
0.2 ± 0.01
|
0.2 ± 0.02
|
-
|
-
|
0.1 ± 0.01
|
cis-sesquisabinene hydrate
|
1545
|
-
|
-
|
0.2 ± 0.05
|
-
|
0.1 ± 0.11
|
-
|
-
|
-
|
-
|
-
|
-
|
elemol
|
1550
|
0.4 ± 0.04
|
0.4 ± 0.04
|
0.4± 0.09
|
0.4 ± 0.06
|
0.6 ± 0.09
|
0.2 ± 0.05
|
0.2 ± 0.04
|
0.2 ± 0.02
|
0.2 ± 0.00
|
0.3 ± 0.04
|
0.2 ± 0.02
|
guaia-3,9-diene
|
1556
|
-
|
-
|
0.1 ± 0.10
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
(E)-nerolidol
|
1564
|
0.6 ± 0.04
|
1.2 ± 0.04
|
0.9 ± 0.36
|
0.8 ± 0.07
|
0.7 ± 0.12
|
1.2 ± 0.13
|
0.3 ± 0.04
|
0.6 ± 0.12
|
0.9 ± 0.11
|
1.5 ± 0.27
|
0.6 ± 0.01
|
palustrol
|
1568
|
-
|
-
|
0.4 ± 0.15
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
caryophyllene alcohol
|
1570
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
spathulenol
|
1577
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
trans-sesquisabinene hydrate
|
1581
|
-
|
0.1 ± 0.05
|
0.2 ± 0.05
|
0.1 ± 0.06
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
caryophyllene oxide3
|
1582
|
11.8 ± 1.18BCD;b
|
11.3 ± 0.85BCD;b
|
10.9 ± 3.38BCDE;a
|
13.9 ± 0.24BC;a
|
22.7 ± 0.45A;a
|
14.4 ± 1.22B;a
|
7.0 ± 1.06E;b
|
9.9 ± 0.78CDE;a
|
9.1 ± 0.74DE;a
|
12 ± 2.03BCD;a
|
9.2 ± 0.11DE;b
|
globulol
|
1583
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
trans-(Z)-α-bisabolene epoxide
|
1586
|
-
|
-
|
0.5 ± 0.16
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
isoaromadendrene epoxide
|
1589
|
0.5 ± 0.10
|
0.5 ± 0.02
|
-
|
0.5 ± 0.06
|
0.8 ± 0.01
|
0.7 ± 0.07
|
0.3 ± 0.01
|
0.5 ± 0.04
|
0.5 ± 0.07
|
0.5 ± 0.08
|
0.4 ± 0.01
|
epi-globulol
|
1590
|
-
|
-
|
-
|
-
|
0.1 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
-
|
viridiflorol
|
1592
|
0.2 ± 0.03
|
0.3 ± 0.05
|
-
|
0.3 ± 0.04
|
0.8 ± 0.04
|
0.2 ± 0.04
|
0.1 ± 0.02
|
0.2 ± 0.00
|
0.3 ± 0.07
|
0.2 ± 0.04
|
-
|
guaiol
|
1596
|
-
|
-
|
0.3 ± 0.09
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
humulene oxide I3
|
1608
|
4.2 ± 0.58BCD;b
|
4.1 ± 0.55BCD;b
|
4.8 ± 1.08BC;a
|
4.9 ± 0.19BC;a
|
9.3 ± 0.46A;a
|
5.2 ± 1.40B;a
|
2.4 ± 0.24D;a
|
3.6 ± 0.32BCD;a
|
3.4 ± 0.28BCD;a
|
4.0 ± 0.58BCD;a
|
3.1 ± 0.03CD;b
|
cedrenol
|
1610
|
0.6 ± 0.11
|
0.1 ± 0.07
|
-
|
0.4 ± 0.03
|
-
|
0.5 ± 0.25
|
0.2 ± 0.00
|
0.3 ± 0.02
|
0.3 ± 0.02
|
0.2 ± 0.02
|
-
|
humulane-1-6-dien-3-ol
|
1613
|
-
|
-
|
0.3 ± 0.03
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
selin-6-en-4-ol3
|
1618
|
1.1 ± 0.02CDE;a
|
1.1 ± 0.23CDE;a
|
0.5 ± 0.17E;b
|
1.2 ± 0.08CD;a
|
0.6 ± 0.05DE;b
|
2.0 ± 0.55A;a
|
0.8 ± 0.23CDE;b
|
0.8 ± 0.11CDE;b
|
1.9 ± 0.06AB;a
|
1.3 ± 0.14BC;a
|
0.7 ± 0.11DE;b
|
13-nor-valenc-1(10)-en-11-one
|
1629
|
-
|
0.2 ± 0.01
|
0.4 ± 0.06
|
0.5 ± 0.05
|
-
|
-
|
-
|
-
|
1.0 ± 0.04
|
0.3 ± 0.34
|
0.2 ± 0.01
|
1-epi-cubenol
|
1627
|
0.4 ± 0.10
|
0.3 ± 0.07
|
0.4 ± 0.06
|
0.3 ± 0.26
|
0.5 ± 0.06
|
0.5 ± 0.10
|
0.2 ± 0.04
|
0.2 ± 0.07
|
0.2 ± 0.00
|
0.4 ± 0.04
|
0.2 ± 0.01
|
γ-eudesmol
|
1631
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
caryophylla-4(14),8(15)-dien-5-ol (unidentified isomer 1)3
|
1633
|
0.7 ± 0.69F;b
|
2.7 ± 0.46AB;b
|
2.5 ± 0.25ABC;b
|
2.6 ± 0.19AB;a
|
2.7 ± 0.27AB;b
|
3.0 ± 0.60A;a
|
1.4 ± 0.15DEF;a
|
0.9 ± 0.10EF;b
|
1.6 ± 0.06CDEF;b
|
2.3 ± 0.13ABCD;b
|
1.7 ± 0.09BCDE;b
|
caryophylla-4(14),8(15)-dien-5-ol (unidentified isomer 2)3
|
1633
|
2.1 ± 0.21ABC;b
|
2.6 ± 0.54AB;b
|
2.8 ± 0.30A;a
|
2.6 ± 0.16AB;b
|
2.7 ± 0.31A;b
|
1.8 ± 0.44BCD;a
|
1.2 ± 0.09D;b
|
1.3 ± 0.04D;b
|
1.2 ± 0.03D;b
|
2.2 ± 0.12ABC;b
|
1.6 ± 0.07CD;b
|
T-cadinol
|
1641
|
-
|
-
|
0.3 ± 0.05
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
cubenol
|
1641
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.4 ± 0.02
|
-
|
-
|
β-eudesmol
|
1649
|
0.2 ± 0.08
|
0.1 ± 0.00
|
-
|
0.2 ± 0.08
|
-
|
0.3 ± 0.09
|
-
|
-
|
-
|
0.2 ± 0.00
|
-
|
α-eudesmol
|
1653
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
neointermedeol
|
1655
|
-
|
-
|
0.3 ± 0.06
|
0.1 ± 0.11
|
0.3 ± 0.02
|
1.2 ± 0.00
|
-
|
-
|
0.2 ± 0.03
|
-
|
0.2 ± 0.00
|
bulnesol
|
1668
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
14-hydroxy-9-epi-(E)-caryophyllene3
|
1670
|
3.8 ± 0.50C;b
|
2.9 ± 0.56C;b
|
5.8 ± 0.62AB;a
|
5.4 ± 0.39B;b
|
7.0 ± 0.53A;b
|
5.5 ± 0.19B;b
|
2.5 ± 0.12C;b
|
3.0 ± 0.28C;b
|
3.6 ± 0.81C;b
|
3.6 ± 0.40C;b
|
2.7 ± 0.21C;b
|
ylangenal
|
1675
|
-
|
1.8 ± 1.66
|
-
|
-
|
0.2 ± 0.02
|
0.2 ± 0.05
|
-
|
-
|
-
|
0.1 ± 0.06
|
-
|
aromadendrene epoxide II
|
1680
|
0.2 ± 0.03
|
0.2 ± 0.03
|
0.2 ± 0.05
|
0.2 ± 0.02
|
0.1 ± 0.01
|
0.1 ± 0.12
|
-
|
0.2 ± 0.01
|
0.1 ± 0.09
|
0.1 ± 0.06
|
0.1 ± 0.02
|
α-bisabolol3
|
1685
|
0.4 ± 0.06E;a
|
1.7 ± 0.36BC;b
|
0.8 ± 0.12DE;a
|
0.4 ± 0.04E;b
|
0.3 ± 0.03E;a
|
1.2 ± 0.06CD;a
|
1.1 ± 0.13CD;a
|
0.6 ± 0.07DE;b
|
5.2 ± 0.49A;a
|
2.2 ± 0.36B;b
|
1.1 ± 0.04CD;a
|
cedr-8-en-13-ol
|
1688
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
juniper camphor
|
1694
|
1.0 ± 0.06
|
1.0 ± 0.24
|
0.4 ± 0.07
|
0.8 ± 0.08
|
0.5 ± 0.02
|
1.8 ± 0.03
|
0.9 ± 0.06
|
0.7 ± 0.07
|
1.0 ± 0.05
|
0.9 ± 0.18
|
0.7 ± 0.02
|
(Z)-α-trans-bergamotol
|
1700
|
-
|
-
|
-
|
-
|
-
|
0.2 ± 0.02
|
-
|
-
|
-
|
-
|
-
|
α-phellandrene dimer
|
1801
|
-
|
-
|
0.1 ± 0.02
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
nootkatone
|
1803
|
-
|
-
|
-
|
-
|
0.2 ± 0.01
|
0.2 ± 0.01
|
-
|
-
|
-
|
-
|
-
|
(E,E)-farnesyl acetate
|
1843
|
-
|
-
|
0.2 ± 0.02
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
hexahydrofarnesylacetone3
|
1845
|
0.6 ± 0.11D;a
|
0.6 ± 0.15D;b
|
1.7 ± 0.24BC;a
|
1.0 ± 0.21D;a
|
1.9 ± 0.11B;a
|
2.3 ± 0.11A;a
|
0.8 ± 0.14D;b
|
1.5 ± 0.05C;b
|
0.7 ± 0.03D;b
|
0.7 ± 0.13D;a
|
0.7 ± 0.01D;b
|
1-hexadecanol
|
1877
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
0.1 ± 0.07
|
0.1 ± 0.05
|
-
|
0.1 ± 0.05
|
(E,E)-farnesyl acetone
|
1918
|
-
|
-
|
0.6 ± 0.12
|
-
|
0.6 ± 0.03
|
0.2 ± 0.06
|
-
|
-
|
-
|
0.1 ± 0.01
|
-
|
m-camphorene
|
1952
|
0.1 ± 0.01
|
-
|
0.2 ± 0.06
|
0.1 ± 0.01
|
-
|
0.1 ± 0.02
|
0.3 ± 0.08
|
0.3 ± 0.03
|
0.1 ± 0.01
|
-
|
0.3 ± 0.00
|
p-camphorene
|
1986
|
0.2 ± 0.10
|
0.1 ± 0.06
|
0.5 ± 0.07
|
0.4 ± 0.07
|
-
|
-
|
0.6 ± 0.11
|
0.6 ± 0.09
|
-
|
-
|
0.6 ± 0.00
|
ethyl hexadecanoate
|
2000
|
-
|
-
|
0.1 ± 0.07
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
-
|
phytol3
|
2112
|
0.5 ± 0.14CD;b
|
0.4 ± 0.18D;b
|
0.8 ± 0.27BCD;b
|
0.4 ± 0.05D;b
|
3.2 ± 0.11A;a
|
2.7 ± 0.04A;b
|
0.9 ± 0.06BC;a
|
0.7 ± 0.19BCD;b
|
1.0 ± 0.07B;b
|
0.8 ± 0.23BCD;a
|
0.9 ± 0.11BC;a
|
cannabidiol3
|
2369
|
23.2 ± 6.13BCDE;a
|
21.8 ± 0.66BCDE;a
|
28.2 ± 1.37ABCD;b
|
20.9 ± 3.94CDE;a
|
16.4 ± 0.36DE;a
|
14.5 ± 1.27E;b
|
35.9 ± 4.68A;b
|
29.6 ± 2.31ABC;a
|
22.2 ± 2.61BCDE;a
|
21.3 ± 10.13CDE;a
|
33.8 ± 0.98AB;a
|
cannabichromene
|
2373
|
0.7 ± 0.36
|
0.7 ± 0.23
|
0.4 ± 0.23
|
0.7 ± 0.25
|
0.7 ± 0.11
|
0.4 ± 0.14
|
1.2 ± 0.39
|
1.1 ± 0.11
|
0.7 ± 0.12
|
0.5 ± 0.29
|
1.1 ± 0.07
|
Δ9-tetrahydrocannabinol
|
2468
|
0.3 ± 0.09
|
0.4 ± 0.06
|
0.5 ± 0.01
|
0.2 ± 0.03
|
0.2 ± 0.00
|
0.2 ± 0.04
|
0.6 ± 0.16
|
0.5 ± 0.04
|
0.3 ± 0.08
|
0.3 ± 0.22
|
0.6 ± 0.01
|
Total identified (%)
|
|
94.5 ± 0.66
|
97.7 ± 0.08
|
98.1 ± 0.63
|
97.4 ± 0.09
|
99.4 ± 0.08
|
92.9 ± 1.03
|
96.9 ± 0.34
|
97.2 ± 0.25
|
95.8 ± 0.86
|
96.1 ± 1.06
|
97.2 ± 0.23
|
Monoterpene hydrocarbons
|
|
4.3 ± 0.71 BCD;a
|
4.1 ± 1.57 BCD;a
|
1.8 ± 0.52 DE;a
|
2.0 ± 0.36 DE;a
|
4.0 ± 0.60 BCD;a
|
1.2 ± 0.15 E;a
|
7.5 ± 0.42 A;a
|
5.7 ± 2.07 AB;a
|
3.7 ± 0.01 BCDE;a
|
2.5 ± 0.85 CDE;a
|
4.7 ± 0.35 BC;a
|
Oxygenated monoterpenes
|
|
0.5 ± 0.10 DE;a
|
0.9 ± 0.34 D;b
|
0.3 ± 0.06 E;a
|
0.2 ± 0.05 E;a
|
0.5 ± 0.07 DE;a
|
0.9 ± 0.15 D;a
|
1.8 ± 0.20 BC;a
|
2.3 ± 0.30 A;a
|
1.4 ± 0.12 C;a
|
0.6 ± 0.06 DE;a
|
2.0 ± 0.10 AB;a
|
Sesquiterpene hydrocarbons
|
|
35.5 ± 2.88 A;a
|
35.6 ± 2.00 A;a
|
29.6 ± 6.37 AB;a
|
35.8 ± 3.03 A;a
|
21.3 ± 0.88 B,a
|
29.7 ± 3.84 AB;a
|
28.5 ± 1.67 AB;a
|
31.8 ± 3.45 AB;a
|
34.5 ± 2.15 A;a
|
36.9 ± 8.42 A;a
|
29.6 ± 1.31 AB;a
|
Oxygenated sesquiterpenes
|
|
|
|
|
|
|
|
|
|
|
|
|
Diterpene hydrocarbons
|
|
|
|
|
|
|
|
|
|
|
|
|
Oxygenated diterpenes
|
|
|
|
|
|
|
|
|
|
|
|
|
Phenylpropanoids
|
|
|
|
|
|
|
|
|
|
|
|
|
Cannabinoids
|
|
|
|
|
|
|
|
|
|
|
|
|
Apocarotenoids
|
|
|
|
|
|
|
|
|
|
|
|
|
Other non-terpene derivatives
|
|
|
|
|
|
|
|
|
|
|
|
|
Extraction yield (% w/w)
|
|
|
|
|
|
|
|
|
|
|
|
|
|